Academic Journal

Study of Mn4Si7 Silicide Alloys Produced Under Different Conditions Using an X-ray Diffractometer

Bibliographic Details
Title: Study of Mn4Si7 Silicide Alloys Produced Under Different Conditions Using an X-ray Diffractometer
Authors: B.D. Igamov, A.I. Kamardin, D.Kh. Nabiev, G.T. Imanova, I.R. Bekpulatov, I.Kh. Turapov, N.E. Norbutaev
Source: Қарағанды университетінің хабаршысы. Физика сериясы, Vol 11830, Iss 2 (2025)
Publisher Information: Karagandy University of the name of academician E.A. Buketov, 2025.
Publication Year: 2025
Subject Terms: crystallization, amorphous, dislocation density, Nuclear and particle physics. Atomic energy. Radioactivity, diffusion, Thermodynamics, QC770-798, QC310.15-319, nonstoichiometric, lattice tension
Description: Mn4Si7 silicide crystals obtained by hot isostatic pressing (HIP) and diffusion methods were studied. As a resultof the research, 11 peaks were identified in the Mn4Si7 crystal obtained by the HIP method, and 14 peaksin the Mn4Si7 crystal obtained by the diffusion method. The crystal size of Mn4Si7 silicide (DHIP) was establishedfrom 8.8∙10–9 m to 3.6∙10–8 m, (DDiff) from 6.2∙10–10 m to 9.1∙10–8 m. It has been established that thelattice tension between the atoms of the Mn4Si7 silicide crystal (εHIP) varies from 0.01 to 0.41, (εDiff) from0.31 to 3.71. The dislocation density on the crystal surface (δHIP) turned out to be from 3.5∙1010 to 3.2∙1012,(δDiff) from 1∙1011 to 3.2∙1014. The degree of crystallization of Mn4Si7 silicide obtained by the (HIP) method is7.02 %, the degree of amorphy is 92.98 %. It has been established that the Mn4Si7 silicide obtained by the diffusionmethod has a degree of crystallization of 9.3 % and a degree of amorphism of 90.7 %. (COD-1530134)(d). It has been established that the degree of crystallization of high-manganese silicide Mn4Si7 is low, and thedegree of amorphy is high due to the fact that Mn and Si are bound in a non-stoichiometric state.
Document Type: Article
ISSN: 2663-5089
2518-7198
DOI: 10.31489/2025ph2/27-34
Access URL: https://doaj.org/article/52df3e9c413f4feb9ace0f9692121cfd
Accession Number: edsair.doi.dedup.....7b0b9a9e972e952385caaadeef8affe2
Database: OpenAIRE
Description
ISSN:26635089
25187198
DOI:10.31489/2025ph2/27-34