Search Results - "константы распределения"

Source: Proceedings of the National Academy of Sciences of Belarus, Chemical Series; Том 59, № 2 (2023); 139-149 ; Известия Национальной академии наук Беларуси. Серия химических наук; Том 59, № 2 (2023); 139-149 ; 2524-2342 ; 1561-8331 ; 10.29235/1561-8331-2023-59-2

Subject Terms: мед, amitraz metabolites, distribution constants, liquid-liquid extraction, high-performance liquid chromatography, mass-spectrometry, honey, метаболиты амитраза, константы распределения, жидкость-жидкостная экстракция, высокоэффективная жидкостная хроматография, масс-спектрометрия

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Relation: https://vestichem.belnauka.by/jour/article/view/812/705; Chapter 41 - Amitraz // Veterinary Toxicology. Basic and Clinical Principles / ed. R. C. Gupta. – 3d ed. – Academic Press, 2018. – P. 525–531. https://doi.org/10.1016/B978-0-12-811410-0.00041-6; Development and validation of modified QuEChERS method coupled with LC–MS/MS for simultaneous determination of cymiazole, fipronil, coumaphos, fluvalinate, amitraz, and its metabolite in various types of honey and royal jelly / W. Zheng [et al.] // J. Chromatogr. B. – 2018. – Vol. 1072. – P. 60–69. https://doi.org/10.1016/j.jchromb.2017.11.011; Determination of amitraz and 2,4-dimethylaniline residues in honey by using LC with UV detection and MS/MS / J.-Z. Xu [et al.] // J. Sep. Science. – 2009. – Vol. 32, iss. 23-24. – P. 4020–4024. https://doi.org/10.1002/jssc.200900437; Teratogenic effects of amitraz, 2,4-dimethylaniline, and paraquat on developing frog (Xenopus) embryos / O. Osano [et al.] // Arch. Environ. Contam. Toxicol. – 2002. – Vol. 43. – P. 42–49. https://doi.org/10.1007/s00244-002-1132-4; Determination of amitraz and its transformation products in pears by ethyl acetate extraction and liquid chromatography–tandem mass spectrometry / N. Tokman [et al.] // J. Chromatogr. A. – 2009. – Vol. 1216, iss. 15. – P. 3138–3146. https://doi.org/10.1016/j.chroma.2009.01.099; Kinetics and mechanism of amitraz hydrolysis in aqueous media by HPLC and GC-MS / E. Corta [et al.] // Talanta. – 1999. – Vol. 48, iss. 1. – P. 189–199. https://doi.org/10.1016/S0039-9140(98)00237-9; Solvent and surfactant enhanced solubilization, stabilization, and degradation of amitraz / C. M. van Eeden [et al.] // J. Environ. Sci. Health, Part B. – 2004. – Vol. B39, N 1. – P. 33–51. https://doi.org/10.1081/PFC-120027437; Показатели безопасности и безвредности для человека продовольственного сырья и пищевых продуктов : ГН от 21.06.2013 № 52 : утв. М-вом здравоохранения Респ. Беларусь 21.06.2013 № 52 // Сборник нормативных документов по продовольственному сырью и пищевым продуктам. – Минск, 2014. – С. 235.; О безопасности пищевой продукции : ТР ТС 021/2011 : принят 09.12.2011 : вступ. в силу 01.07.2013 / Совет Евраз. эконом. комиссии. – Минск : Энергопресс, 2021. – 144 с.; Commission Regulation (EU) № 37/2010 of 22 December 2009 on pharmacologically active substances and their classification regarding maximum residue limits in foodstuffs of animal origin // Off. J. of the European Union. – 2010. – N L15. – P. 1–72. https://doi.org/10.3000/17252555.L_2010.015.eng; Gao, X. Simultaneous determination of amitraz, chlordimeform, formetanate and their main metabolites in human urine by high performance liquid chromatography-tandem mass spectrometry / X. Gao, Y. Tan, H. Guo // J. Chromatogr. B. – 2017. – Vol. 1052 – P. 27–33. https://doi.org/10.1016/j.jchromb.2017.03.004; Honey: Chemical composition, stability and authenticity / P. M. da Silva [et al.] // Food Chem. – 2016. – Vol. 196. – P. 309–323. http:// doi.org/10.1016/j.foodchem.2015.09.051; Development and validation of a method for the analysis of total amitraz in fruit and honey with quantification by gas chromatography-mass spectrometry / M. Caldow [et al.] // Food Addit. Contam. – 2007. – Vol. 24, iss. 3. – P. 280–284. https://doi.org/10.1080/02652030601013638; Analysis of ‘‘Amitraz (sum)’’ in pears with incurred residues – Comparison of the approach covering the individual metabolites via LC–MS/MS with the approach involving cleavage to 2,4-dimethylaniline / J. Hepperle [et al.] // Food Chem. – 2015. – Vol. 166. – P. 240–247. https://doi.org/10.1016/j.foodchem.2014.06.003; Simultaneous determination of amitraz and its metabolite residue in food animal tissues by gas chromatography-electron capture detector and gas chromatography–mass spectrometry with accelerated solvent extraction / H. Yu [et al.] // Journal of Chromatography B. Analyt. Technol. Biomed. Life Sci.– 2010. – Vol. 878, iss. 21. – P. 1746–1752. https://doi.org/10.1016/j.jchromb.2010.04.034; Extraction and clean-up methods for the determination of amitraz total residues in beeswax by gas chromatography with electron capture detection / J. J. Jiménez [et al.] // Anal. Chim. Acta. – 2004. – Vol. 524, iss. 1–2. – P. 271–278. https://doi.org/10.1016/j.aca.2004.03.039; Determination of amitraz and its metabolites in whole blood using solid-phase extraction and liquid chromatography–tandem mass spectrometry / H. Guo [et al.] // J. Chromatogr. B. Analyt. Technol. Biomed. Life Sci. – 2014. – Vol. 951–952. – P. 89–95. https://doi.org/10.1016/j.jchromb.2014.01.027; Simultaneous determination of nine acaricides and two metabolites in comb honey by LC/MS/MS / Y. Ohba [et al.] // Food Addit. Contam.: Part A Chem. Anal. Control Expo. Risk Assess. – 2018. – Vol. 35, iss. 12. – P. 2375–2386. https://doi.org/10.1080/19440049.2018.1539252; Multi-residue method for the determination of pesticides and pesticide metabolites in honeybees by liquid and gas chromatography coupled with tandem mass spectrometry – Honeybee poisoning incidents / T. Kiljanek [et al.] // J. Chromatogr. А. – 2016. – Vol. 1435. – P. 100–114. https://doi.org/10.1016/j.chroma.2016.01.045; Мёд натуральный. Определение массовой доли инсектицидов методом газовой хроматографии с масс-спектрометрическим детектированием : ГОСТ 34889-2022. – Введ. 31.08.2022. – Минск : Евраз. совет по стандартизации, метрологии и сертификации, 2022. – 11 с.; Разработка и валидация методики определения амитраза в меде высокоэффективной жидкостной хроматографией с масс-спектрометрическим детектированием / А. Г. Полоневич [и др.] // Вес. Нац. акад. навук Беларусi. Сер. хiм. навук. – 2022. – Т. 58, № 4. – С. 387–397. https://doi.org/10.29235/1561-8331-2022-58-4-387-397; Amitraz (Ref: ENT 27967) [Electronic resource] // PPDB: Pesticide Properties DataBase. – Mode of access: http://sitem.herts.ac.uk/aeru/ppdb/en/Reports/30.htm. – Date of access: 30.12.2022.; Solubilities of pesticide chemicals in water. Part II: Data compilation / Shiu W. Y. [et al.] // Reviews of Environmental Contamination and Toxicology / eds.: G.W. Ware, H.N. Niggs, A. Bevenue. Springer, New York, 1990. – Vol. 116. – P. 15–187. https://doi.org/10.1007/978-1-4612-3434-0_2; New QSPR study for the prediction of aqueous solubility of drug-like compounds / P. R. Duchowicz [et al.] // Bioorg. Med. Chem. – 2008. – Vol. 16, iss. 17. – P. 7944–7955. https://doi.org/10.1016/j.bmc.2008.07.067.; Amitraz [Electronic resource] // PubChem. – Mode of access: https://pubchem.ncbi.nlm.nih.gov/compound/Amitraz. – Date of access: 30.12.2022.; https://vestichem.belnauka.by/jour/article/view/812

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https://doi.org/10.29235/1561-8331-2023-59-2-139-149

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7

Academic Journal

Organic solvent extraction of anabolic steroids from aqueous solutions ; Экстракция анаболических стероидов органическими растворителями из водных растворов

Authors: S. M. Leschev, Yu. G. Pakhadnia, O. N. Tchekhovskaya, A. A. Ahabalayeu, M. F. Zayats, С. М. Лещев, Ю. Г. Походня, О. Н. Чеховская, А. А. Агабалаев, М. Ф. Заяц

Source: Proceedings of the National Academy of Sciences of Belarus, Chemical Series; Том 59, № 4 (2023); 302-311 ; Известия Национальной академии наук Беларуси. Серия химических наук; Том 59, № 4 (2023); 302-311 ; 2524-2342 ; 1561-8331 ; 10.29235/1561-8331-2023-59-4

Subject Terms: газовая хромато-масс-спектрометрия, metabolites, urine, extraction, partition ratios, gas chromatography-mass spectrometry, метаболиты, моча, экстракция, константы распределения

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Relation: https://vestichem.belnauka.by/jour/article/view/848/720; Рожкова, Е. И. Анаболические стероиды как допинги в спорте / Е. И. Рожкова, Р. З. Сейфулла // Казан. мед. журн. – 2009. – Т. 90, № 4. – С. 601–604.; Грундинг, П. Анаболические стероиды / П. Грундинг, М. Бахманн. – М.: Спорт, 1994. – 92 с.; Фармакология спорта / Н. А. Горчакова [и др.]; под общ. ред. С. А. Олейника, Л. М. Гуниной, Р. Д. Сейфуллы. – К.: Олимп. лит., 2010. – 640 с.; Kuhn, C. M. Anabolic steroids / C. M. Kuhn // Recent Progress in Hormone Research. – 2002. – Vol. 57, № 1. – P. 411–434. https://doi.org/10.1210/rp.57.1.411; Kicman, A. T. Anabolic steroids in sport: biochemical, clinical and analytical perspectives / A. T. Kicman, D. B. Gower // Ann. Clin. Biochem. – 2003. – Vol. 40, № 4. – P. 321–356. https://doi.org/10.1258/000456303766476977; Bahrke, M. S. Abuse of anabolic androgenic steroids and related substances in sport and exercise / M. S. Bahrke, C. E. Yesalis // Curr. Opin. Pharmacol. – 2004. – Vol. 4. – P. 614–620. https://doi.org/10.1016/j.coph.2004.05.006; Determination of reference intervals for urinary steroid profiling using a newly validated GC-MS/MS method / W. de Jong [et al.] // Clin. Chem. Lab. Med. (CCLM). – 2018. – Vol 56, iss. 1. – P. 103–112. https://doi.org/10.1515/cclm-2016-1072; Gas chromatography/mass spectrometry (GC/MS) remains a pre-eminent discovery tool in clinical steroid investigations even in the era of fast liquid chromatography tandem mass spectrometry (LC/MS/MS) / N. Krone [et al.] // J. Steroid Biochem. Mol. Biol. – 2010. –Vol. 121, Iss. 3–5. – P. 496–504. https://doi.org/10.1016/j.jsbmb.2010.04.010; Doping control analysis of anabolic steroids in equine urine by gas chromatography-tandem mass spectrometry / A. S. Y. Wong [et al.] // Drug Test. Analysis. – 2017. – Vol. 9, № 9. – P. 1320–1327. https://doi.org/10.1002/dta.2090; Determination of nandrolone metabolites in human urine: comparison between liquid chromatography/tandem mass spectrometry and gas chromatography/mass spectrometry / F. Buiarelli [et. al.] // Rapid Commun. Mass Spectrom. – 2010. – Vol. 24, № 13. – P. 1881–1894. https://doi.org/10.1002/rcm.4583; Determination of four anabolic steroid metabolites by gas chromatography/mass spectrometry with negative ion chemical ionization and tandem mass spectrometry / M. H. Choi [et al.] // Rapid Commun. Mass Spectrom. – 1998. – Vol. 12, № 22. – P. 1749–1755. https://doi.org/10.1002/(sici)1097-0231(19981130)12:223.0.co;2-s; A Method for Determination of One Hundred Endogenous Steroids in Human Serum by Gas Chromatography-Tandem Mass Spectrometry / M. Hill [et al.] // Physiol. Res. – 2019. – Vol. 68. – P. 179–207. https://doi.org/10.33549/physiolres.934124; Shackleton, C. GC/MS in Recent Years Has Defined the Normal and Clinically Disordered Steroidome: Will It Soon Be Surpassed by LC/Tandem MS in This Role? / C. Shackleton, O. J. Pozo, J. Marcos // Journal of the Endocrine Society. – 2018. – Vol. 2, iss. 8. – P. 974–996. https://doi.org/10.1210/js.2018-00135; Hydrolysis of conjugated steroids by the combined use of beta-glucuronidase preparations from helix pomatia and ampullaria: determination of urinary cortisol and its metabolites / H. Shibasaki [et al.] // Steroids. – 2001. – Vol. 66, iss. 11. – P. 795–801. https://doi.org/10.1016/s0039-128x(01)00118-0; Catlin, D. H. Detection of norbolethone, an anabolic steroid never marketed, in athletes’ urine / D. H. Catlin, B. D. Ahrens, Y. Kucherova // Rapid Commun. Mass Spectrom. – 2002. – Vol. 16, iss. 13. – P. 1273–1275. https://doi.org/10.1002/rcm.722; Tetrahydrogestrinone: discovery, synthesis, and detection in urine / D. H. Catlin [et al.] // Rapid Commun. 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Derivatization procedures for gas chromatographic–mass spectrometric determination of xenobiotics in biological samples, with special attention to drugs of abuse and doping agents / J. Segura, R. Ventura, C. Jurabo // J. Chromatogr. B. – 1998. – Vol. 713, iss. 1. – P. 61–90. https://doi.org/10.1016/s0378-4347(98)00089-9; McDonald, J. G. Steroid profiling by gas chromatography-mass spectrometry and high performance liquid chromatography-mass spectrometry for adrenal diseases / J. G. McDonald, S. Matthew, R. J. Auchus // Horm Cancer. – 2011. – Vol. 2, № 6. – P. 324–332. https://doi.org/10.1007/s12672-011-0099-x; Graf, V. Hydrolysis of steroid glucuronides with ß-glucuronidase preparations from bovine liver, Helix pomatia and E. coli / V. Graf, E. Furuya, O. Nishikaze // Clin. Chem. – 1977. – Vol. 23, iss. 3. – P. 532–535. https://doi.org/10.1093/clinchem/23.3.532; https://vestichem.belnauka.by/jour/article/view/848

Availability: https://vestichem.belnauka.by/jour/article/view/848
https://doi.org/10.29235/1561-8331-2023-59-4-302-311

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8

Academic Journal

Экстракция хлорамфеникола органическими растворителями

Authors: Сергей Михайлович Лещёв, Елена Ильинична Полянских

Source: Журнал Белорусского государственного университета: Химия, Iss 2, Pp 35-41 (2023)

Subject Terms: хлорамфеникол, жидкость-жидкостная экстракция, константы распределения, высокоэффективная жидкостная хроматография, тандемная масс-спектрометрия, пищевая продукция, Chemistry, QD1-999

Relation: https://journals.bsu.by/index.php/chemistry/article/view/5722; https://doaj.org/toc/2520-257X; https://doaj.org/toc/2617-3980; https://doaj.org/article/79fa9790e4a84f2bb731ceab001d6b86

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9

Academic Journal

Extraction of acid type penicillins by organic solvents ; Экстракция пенициллинов кислотного типа органическими растворителями

Authors: A. G. Polonevich, S. M. Leschev, A. I. Palianskikh, L. L. Belyshava, А. Г. Полоневич, С. М. Лещев, Е. И. Полянских, Л. Л. Белышева

Source: Proceedings of the National Academy of Sciences of Belarus, Chemical Series; Том 56, № 3 (2020); 284-292 ; Известия Национальной академии наук Беларуси. Серия химических наук; Том 56, № 3 (2020); 284-292 ; 2524-2342 ; 1561-8331 ; 10.29235/1561-8331-2020-56-3

Subject Terms: масс-спектрометрия, distribution constants, acid type penicillins, high-performance liguid chromatography, mass spectrometry, константы распределения, пенициллины кислотного типа, высокоэффективная жидкостная хроматография

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Relation: https://vestichem.belnauka.by/jour/article/view/596/573; О безопасности молока имолочной продукции: ТРТС 033/2013: принят 09.10.2013: вступ. в силу 01.05.2014 / Совет Евраз. экон. комис. - Минск: Энергопресс, 2014. - 191 с.; О максимально допустимых уровнях остатков ветеринарных лекарственных средств (фармакологически активных веществ), которые могут содержаться в непереработанной пищевой продукции животного происхождения, в том числе в сырье, и методиках их определения [Электронный ресурс] : решение Коллегии Евраз. экон. комис. 13.02.2018 № 28 // КонсультантПлюс. Беларусь / ООО «Юрспектр», Нац. центр правовой информ. Респ. Беларусь. -Минск, 2020.; О безопасности мяса и мясной продукции: ТР ТС 034/2013: принят 09.10.13: вступ. в силу 01.05.14 / Евраз. экон. комис. - Минск: Энергопресс, 2014. - 103 с.; Tyczkowska, K. L. Solvent degradation of cloxacillin in vitro. Tentative identification of degradation products using thermospray liquid chromatography-mass spectrometry / K. L. Tyczkowska, R. D. Voyksner, A. L. Aronson // Journal of Chromatography. - 1992. - Vol. 594, N 1-2. - P. 195-201. https://doi.org/10.1016/0021-9673(92)80330-w_; Hou, J. P. P-Lactam Antibiotics: Their Physicochemical Properties and Biological Activities in Relation to Structure / J. P. Hou, J. W. Poole // Journal of Pharmaceutical Sciences. - 1971. - Vol. 60, N 4. - P. 503-532. https://doi.org/10.1002/jps.2600600402; Deshpande, A. D. Degradation of P-Lactam Antibiotics / A. D. Deshpande, K. G. Baheti, N.R. Chatterjee // Current Science. - 2004. - Vol. 87, N 12. - P. 1684-1695.; Егоров, Н. С. Основы учения об антибиотиках / Н. С. Егоров. - М.: Высш. шк., 1998. - 447 с.; Purification of penicillin: pat. US 2503216 / G. J. Gino, R. A. Wilson, E. A. Anderson. - Publ. date 04.04.1950.; Recovery of biosynthetic penicillins / M. I. Yakhkind [et al.] // Advances in medicine and biology / ed. Leon V. Berhardt. - Nova Science Publishers INC., 2014. - Vol. 79. - P. 87-128.; Becker, M. Residue analysis of 15 penicillins and cefalosporins in bovine muscle, kidney and milk by liquid chromatography-tandem mass spectrometry / M. Becker, E. Zittlau, M. Petz // Analytica Chimica Acta. - 2004. - Vol. 520, N 1-2. -P. 19-32. https://doi.org/10.1016/j.aca.2004.04.022; Determination of penicillins residues in livestock and marine products by LC/MS/MS / Ji Young Song [et al.] // World academy of science, engineering and technology. - 2011. - Vol. 57. - P. 809-811.; Multi residue determination of the penicillins regulated by European Union, in bovine, porcine and chicken muscle, by LC-MS/MS / C. A. Macarov [et al.] // Food Chemistry. - 2012. - Vol. 135. - Р. 2612-2621. https://doi.org/10.10167j.food-chem.2012.06.126; Полянских, Е. И. Методика контроля остаточного содержания антибиотиков пенициллиновой группы в продукции животного происхождения / Е. И. Полянских,А. Г. Полоневич, Л. Л. Белышева // Хим. безопасность. - 2017. -Т. 1, № 1. - С. 200-215.; Physicochemical properties of P-lactam antibiotics: oil-water distribution / A. Tsuji [et al.] // Journal of Pharmaceutical Sciences. - 1977. - Vol. 66, N 12. - P. 1675-1679. https://doi.org/10.1002/jps.2600661205; Lee, S. C. Physical and reactive extraction equilibria of penicillin G in a hydrogen-bond acceptor solvent system / S. C. Lee // Biotechnol Prog. - 2006. - Vol. 22, N 3. - P. 731-736. https://doi.org/10.1021/bp050380y; Rapson, H. D. C. Ionisation constants of some penicillins and of their alkaline and penicillinase hydrolysis products / H. D. C. Rapson, A. E. Bird // Journal of Pharmacy and Pharmacology. - 1963. - Vol. 15, N S1. - P. 222T-231T. https://doi.org/10.1111/j.2042-7158.1963.tb11216.x; Hou, J. P. The amino acid nature of ampicillin and related penicillins / J. P. Hou, J. W. Poole // J. Pharmaceuticals Sciences. 1969. - Vol. 58, N 12. - P. 1510-1515. https://doi.org/10.1002/jps.2600581219; https://vestichem.belnauka.by/jour/article/view/596